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The only way to make sure is the use of the
highest quality fuel gas, the highest quality zero gas, the most
accurate span gas and enough time to let an analyzer completely
drift out in a low range before calibration. A good FID analyzer
practically is nearly drift free. What you see drifting in a
THC analyzer is hydrocarbons building up by condensing in the
system, forming a hang up (also called a memory effect). Again:
Clean FID analyzers are nearly drift free.
Only a contaminated or defective FID analyzer
(and sample train) drifts. The condensed hydrocarbons tend to
accumulate on (in) sample-wetted materials like the sample lines,
tubes, filters, valves and diaphragms. Once a hydrocarbon hang
up has gotten old, it is difficult and time consuming to clean
it off. In most cases, clean air, heat and your valuable time
are the only tools.
Calibrate your analyzer with zero gas and
span gas as often as possible. When the circumstances allow,
do it once (or twice) per day. The more often you calibrate,
the quicker you see when a hang up starts to build up. When you
get repeatable zero and span calibration results, your measuring
results will also be correct and repeatable.
Once you finished your measuring campaign
or project, do not turn your analyzer off immediately! First,
backpurge the sample filter for a few seconds. Then let your
analyzer run clean by sampling low contaminated ambient air or
zero gas for at least 60 minutes. Running your analyzer clean
helps to remove residual hydrocarbons and other contaminants,
which have been brought into the analyzer during sampling. These
hydrocarbons would otherwise condense during the cool down period
and contaminate the sample-wetted components. |